Engle Lab @EngleLab
catalysis, reaction discovery, and samoyed sled racing @scrippsresearch. views our own. englelab.com La Jolla, San Diego Joined September 2015-
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Check out the @scrippsresearch NMR Core live tour w/ the Engle lab's own @madisonfayw! youtube.com/live/03V1z_MJy…
Why did Sourav Sekhar Bera (@SouravSekharBe2) choose chemistry as a career? Find out on his #IntroducingAngewandte page on the occasion of his first article as a submitting corresponding author in Angewandte Chemie (doi.org/10.1002/anie.2…): onlinelibrary.wiley.com/doi/10.1002/an…
@JonathanLKuo @avrlisboa thank you @JonathanLKuo! It was fun to follow the trail of clues from 10-years of product crystal structures to something measurable in the end!
What's the secret sauce that makes 8-aminoquinoline (AQ) a good directing group?🧐 @avrlisboa's new paper examines w/ 200+ X-ray structures + DFT + competition exps. Spoiler: it's locked in 🔐 sciencedirect.com/science/articl…
Excited to share our new @ACSChemRev pub w/ the @bfshi lab at Zhejiang U! We survey enantioselective C–H functionalization with first-row TMs: mechanisms, ligand design, and applications across Co, Ni, Fe, and Cu. Check it out! 🔗 tinyurl.com/58v48tkn
Bench-stable Ni(II) precats w/ superb solubility that activate cleanly & work ↔️ Suzuki–Miyaura, Buchwald–Hartwig, Miyaura borylation, and olefin difunctionalization. The final version of Nana & Aimee's Ni(C6F5)2 paper is out @Orgmet_ACS #BMSChemistry tinyurl.com/4xt8dw94
We found an unexpected byproduct in our cyclopropanation work. X-ray structure ➡️ isoxazoline N-oxide. We optimized for this [3+2] product, figured out the scope, and now share the final story in @JOC_OL 🔗 tinyurl.com/4vvc5c2j
Bidentate DGs are a powerful tool for controlling reactivity and selectivity in π-bond functionalization—and for mechanistic elucidation! Great seeing growing adoption and pleased to team up w/ @TaehoKang6's lab to review the state of play! @angew_chem tinyurl.com/2cmnn2r8
Together w/ @pengliu_group & #BMSChemistry we inverted the classical selectivity paradigm of organometallic additions to Michael acceptors, achieving enantioselective anti-Michael addition of (hetero)aryl groups under Pd/PhTRAP catalysis. tinyurl.com/3r4yrjd2
5+ years developing stable Ni catalysts—and always battling poor solubility! Inspired by the inorg chem literature, our lab w/ a team from @UCSDChemBiochem & #BMSChemistry now report [Ni(C6F5)2] precats w/ superb solubility, stability & convenience. tinyurl.com/yvm7v7yf
The final peer-reviewed version of this collaborative study w/ #BMSChemistry, @pengliu_group, and @GuteGroup is online @ACSCentSci. Alkyl-9-BBN reagents have quickly proven simple and surprisingly effective in numerous 3-component couplings in the lab! pubs.acs.org/doi/10.1021/ac…
C(sp3)-C(sp3) couplings w/o radicals? 🧐 We introduce alkyl-9-BBN reagents to the 3-component coupling party 🎉, enabling access to new encoded cyclooctene monomers for ROMP 🧵 w/ @pengliu_group @GuteGroup @ChemRxiv: tinyurl.com/4fh49ke5 🧪 #TeamNickel #PolymerChem
The final peer-reviewed version of our collaborative study w/ #BMSChemistry, @EnamineLtd, @pengliu_group, & the Blackmond lab developing a flexible directing group for expanded scope in olefin hydroamination is online @J_A_C_S. Bravo @avrlisboa and team! pubs.acs.org/doi/10.1021/ja…
🔧 In a mechanism🔁method tour de force, @avrlisboa & team show that a flexible directing group dramatically improves Pd-catalyzed functionalization of hindered olefins, leading to >115× rate boost and expanded scope. @ChemRxiv tinyurl.com/34rx6w9v @pengliu_group @EnamineLtd
Honored to play a small part in this seminal study—putting Pd(COD)(DQ) to use in a tricky C–N coupling, setting the stage for high-throughput SuFEx. Great to collaborate with molecular glue discovery masters upstairs!
What a thrill to see this out! Our prospective, scalable, and target-centric solution for molecular glue discovery. More thoughts and details here: linkedin.com/posts/activity… Paper here: nature.com/articles/s4158…
The final peer-reviewed version of our Ni(DQ)2 study hit the presses @Orgmet_ACS earlier this month. Update regarding commercial availability coming soon! pubs.acs.org/doi/10.1021/ac…
The newest chapter in air-stable Ni(0): Ni(DQ)2 @ChemRxiv pre-print: tinyurl.com/yhzufye8 @HarryHe88239850 @SongLinLab #BMSChemistry
Hey @Support @Safety @X, Our lab account @BaranLabReads was suddenly suspended, but we have exciting science to share! Appeal was submitted can you please help? Calling on our science collaborators & friends to please RT for visibility. @scrippsresearch
Now online and open access: Article by @MykhailiukChem @pengliu_group K. Barry Sharpless, @EngleLab & co-workers Alkyl sulfonyl fluorides as ambiphiles in the stereoselective palladium(II)-catalysed cyclopropanation of unactivated alkenes nature.com/articles/s4416…
The final version of @YilinCao_chem's study, reporting a unique approach to olefin cyclopropanation w/ Alkyl-SO2F compounds is now online in @NatureSynthesis! nature.com/articles/s4416…
The rise of SuFEx has focused a bright spotlight 🔦 on synthesis of RSO2F compounds. What reactivity beyond SuFEx do these compounds possess and how can we unlock it? 🔐 @YilinCao_chem and team have the answer.🔎 tinyurl.com/bp5j6zkk
🔧 In a mechanism🔁method tour de force, @avrlisboa & team show that a flexible directing group dramatically improves Pd-catalyzed functionalization of hindered olefins, leading to >115× rate boost and expanded scope. @ChemRxiv tinyurl.com/34rx6w9v @pengliu_group @EnamineLtd
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